Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Fluoroisatin → 5-fluoro-1,3-dihydro-2H-indol-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Fluoroisatin | HCID 236566 | — |
| 용매 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 생성물 | 5-fluoro-1,3-dihydro-2H-indol-2-one | HCID 3731012 | — |
반응 단계
5-Fluoroisatin (8.2 g) was dissolved in 50 mL of hydrazine hydrate and refluxed for 1.0 hr. The reaction mixtures were then poured in ice water. The precipitate was then filtered, washed with water and dried in a vacuum oven to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06855730B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-85f8d0a13c1741908216e141c66ffd9d |
| 출처 메모 | uspto-grants-2005_02 |