Ammonium Hydroxide → 2-Oxoindoline-5-sulfonamide
반응식
Cl[S:2]([C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[NH:10][C:9](=[O:14])[CH2:8]2)(=[O:4])=[O:3].[OH-].[NH4+:16]>C(O)C>[NH2:16][S:2]([C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[NH:10][C:9](=[O:14])[CH2:8]2)(=[O:4])=[O:3]참가 물질
4
실험 절차
5-Chlorosulfonyl-2-oxindole (2.1 g) was added to 10 mL of ammonium hydroxide in 10 mL of ethanol and stirred at room temperature overnight. The mixture was concentrated and the solid collected by vacuum filtration to give 0.4 g (20% yield) of the title compound as an off-white solid.
후처리
- concentrationThe mixture was concentrated
- filtrationthe solid collected by vacuum filtration
출처 및 근거
- ORD 기록
- ord-2520af5761ac4f8b8d7b07549287ce02
- 출처 데이터셋
- uspto-grants-2005_02
- 특허 번호
- US06855730B2
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