4-Nitrobenzoic Acid → Methyl 2-[(4-nitrobenzoyl)amino]benzoate

HRID 2433

반응식

HRID 2433 반응식
[C:1]([O:10][CH3:11])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[N+:12]([C:15]1[CH:23]=[CH:22][C:18]([C:19](O)=[O:20])=[CH:17][CH:16]=1)([O-:14])=[O:13]>>[N+:12]([C:15]1[CH:16]=[CH:17][C:18]([C:19]([NH:4][C:3]2[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=2[C:1]([O:10][CH3:11])=[O:9])=[O:20])=[CH:22][CH:23]=1)([O-:14])=[O:13]

참가 물질

3

반응물 2

HCID 61084-Nitrobenzoic AcidHCID 8635Methyl Anthranilate

생성물 1

HCID 787257Methyl 2-[(4-nitrobenzoyl)amino]benzoate수율 72.9%

실험 절차

Using methyl anthranilate (3.02 g, 20.0 mmol) and 4-nitrobenzoic acid (3.67 g, 22.0 mmol), the procedure of Reference Example 16 was repeated to obtain 4.20 g (72.9%) of the title compound in the form of light yellow prism crystals.

출처 및 근거

ORD 기록
ord-0da5c45fb1f94fe58e6de013c7b3d1b3
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05728835

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