참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Malononitrile | HCID 8010 | — |
| 반응물 | Triethyl orthoacetate | HCID 66221 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | (1-Ethoxyethylidene)malononitrile | HCID 79450 | 86% |
반응 단계
A mixture of malononitrile (5.0 g, 76 mmol), (EtO)3CCH3 (14.8 g, 91 mmol) and CH3COOH (1 mL) was stirred at 80° C. for 45 min. Then the mixture was cooled to room temperature and filtered to give 2-(1-ethoxy-ethylidene)-malononitrile (8.9 g, yield 86%) as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08653089B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_02 |
|---|
| ORD ID | ord-d1ed5381a1de43f9a4367b9d791ffd75 |
|---|
| 출처 메모 | uspto-grants-2014_02 |
|---|
