Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Fluoro-2-iodobenzoic acid → 5-Iodo-2-[1,2,3]triazol-2-yl-benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Fluoro-2-iodobenzoic acid | HCID 13158583 | — |
| 반응물 | 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086948 | — |
| 생성물 | 5-Iodo-2-[1,2,3]triazol-2-yl-benzoic acid | HCID 67086732 | — |
반응 단계
The title compound was prepared in a manner analogous to Intermediate 1, substituting 2-bromo-5-iodobenzoic acid for 5-fluoro-2-iodo-benzoic acid in Step A. 1H NMR (400 MHz, CD3OD): 8.09 (d, J=2.0, 1H), 8.03-7.97 (m, 1H), 7.95-7.86 (m, 3H), 7.53 (d, J=8.4, 1H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08653263B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-d9a258a52f604289a23b3b751f2da77e |
| 출처 메모 | uspto-grants-2014_02 |