Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Nitrobenzoic acid → N-[3-(methylsulfanyl)phenyl]-3-nitrobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Nitrobenzoic acid | HCID 8497 | — |
| 반응물 | Benzenamine, 3-(methylthio)- | HCID 15693 | — |
| 생성물 | N-[3-(methylsulfanyl)phenyl]-3-nitrobenzamide | HCID 895917 | 94.6% |
반응 단계
Using 3-methylthioaniline (2.1 ml, 16.5 mmol) and 3-nitrobenzoic acid (2.64 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 4.09 g (94.6%) of the title compound in the form of light yellow needle crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728835 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-c16cf1c3e2df4892b6f3150e9b21bcaf |
| 출처 메모 | uspto-grants-1998_03 |