Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitrobenzoyl chloride → N-(1,3-benzodioxol-5-yl)-4-nitrobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| 반응물 | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
| 생성물 | N-(1,3-benzodioxol-5-yl)-4-nitrobenzamide | HCID 674221 | 87.2% |
반응 단계
Using 3,4-methylenedioxyaniline (1.44 g, 10.5 mmol) and 4-nitrobenzoyl chloride (1.86 g, 10.0 mmol), the procedure of Reference Example 11 was repeated to obtain 2.49 g (87.2%) of the title compound in the form of yellow crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728835 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-b04fe9c2f1da4526a30f3f2067ac49b1 |
| 출처 메모 | uspto-grants-1998_03 |