참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 1,4-Dimethyl-1H-pyrazole-3-carboxylic acid | HCID 5325685 | — |
| 생성물 | 1,4-Dimethyl-1H-pyrazole-3-carbonyl chloride | HCID 58356380 | — |
반응 단계
Thionyl chloride (4 ml) was added to 1,4-dimethyl-1H-pyrazole-3-carboxylic acid (0.5 g) and the reaction was heated at 80° C. for 2 h. Further thionyl chloride (2 ml) was added and the reaction was heated at 80° C. for 1 h. The reaction was evaporated, then azeotroped with toluene to give title compound, 511 mg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08658635B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_02 |
|---|
| ORD ID | ord-45674eb3d94748a3b78460a3aeb10509 |
|---|
| 출처 메모 | uspto-grants-2014_02 |
|---|
