반응식
[C:1]([O:4][CH2:5][C:6]([OH:8])=O)(=[O:3])[CH3:2].Cl.[NH2:10][CH2:11][C:12]1[C:17]([Cl:18])=[N:16][CH:15]=[CH:14][N:13]=1>>[C:1]([O:4][CH2:5][C:6]([NH:10][CH2:11][C:12]1[C:17]([Cl:18])=[N:16][CH:15]=[CH:14][N:13]=1)=[O:8])(=[O:3])[CH3:2]참가 물질
3
실험 절차
According to the procedure described in example 13 step 13a acetoxyacetic acid (0.667 g) and 2-aminomethyl-3-chloropyrazine hydrochloride (content 77%; 0.81 g) gave 2-((3-chloropyrazin-2-yl)methylamino)-2-oxoethyl acetate (0.99 g) after purification by column chromatography (silica gel; gradient of dichloromethane to dichloromethane/ethyl acetate 1/1).
출처 및 근거
- ORD 기록
- ord-c13c3b2d8fe947b4acaf0a37564f1b7a
- 출처 데이터셋
- uspto-grants-2014_02
- 특허 번호
- US08658794B2
연결된 노트
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