Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 24613생성일: 2026년 10월 23일
3,3-Diphenylpropylamine → Benzyl 4-(3-chlorophenyl)-3-(3,3-diphenylpropylcarbamoyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
https://huagongshe.com/ko/reaction/24613
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3,3-Diphenylpropylamine | HCID 79698 | — |
| 반응물 | 5-benzyl 1-(4-nitrophenyl) 6-(3-chlorophenyl)-2-methoxy-4-methyl-6H-pyrimidine-1,5-dicarboxylate | HCID 69745932 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Benzyl 4-(3-chlorophenyl)-3-(3,3-diphenylpropylcarbamoyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate | HCID 15546109 | — |
반응 단계
10 ml of acetonitrile was added to a mixture of 200 mg (0.373 mmol) of 5-benzyl 1-(4-nitrophenyl) 6-(3-chlorophenyl)-2-methoxy-4-methyl-6H-pyrimidine-1,5-dicarboxylate and 78.9 mg (0.373 mmol) of 3,3-diphenylpropylamine, and they were stirred at 60° C. for 30 minutes. The solvent was evaporated under reduced pressure to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06855716B2 |
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| 출처 데이터셋 | uspto-grants-2005_02 |
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| ORD ID | ord-74147c16a95240d69ee024fbc23bdbd2 |
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| 출처 메모 | uspto-grants-2005_02 |
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