Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(Phenylthio)acetic acid → (Phenylthio)acetyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (Phenylthio)acetic acid | HCID 59541 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | (Phenylthio)acetyl chloride | HCID 4063350 | — |
반응 단계
To a solution of 5.0 g of (phenylthio)acetic acid in 20 ml of toluene under nitrogen was added 5.2 ml of oxalyl chloride in four portions. The solution was stirred at room temperature for about twenty hours and then concentrated in vacuo to the oily title compound, which was used in subsequent reactions without further purificaton or characterization.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04704386 |
| 출처 데이터셋 | uspto-grants-1987_11 |
| ORD ID | ord-9ef97c2bf9824e38b8c136f32ff6aa57 |
| 출처 메모 | uspto-grants-1987_11 |