참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chlorine | HCID 24526 | — |
| 반응물 | 4-Fluoro-3-nitrobenzotrifluoride | HCID 67778 | — |
| 생성물 | Benzene, 2-chloro-1-fluoro-4-(trifluoromethyl)- | HCID 157153 | — |
반응 단계
In a continuous process, about 8 parts per hour of 4-fluoro-3-nitrobenzotrifluoride vapors and about 15 parts per hour of chlorine gas were passed simultaneously through a vapor phase reactor maintained at a temperature of about 320° C. and the reaction product vapors were condensed and collected. The process was continued until about 40 parts of 4-fluoro-3-nitrobenzotrifluoride had been passed through the reactor, yielding about 36.3 parts of 3-chloro-4-fluorobenzotrifluoride product. The structure of the product was confirmed by spectral analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04704483 |
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| 출처 데이터셋 | uspto-grants-1987_11 |
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| ORD ID | ord-6e8d9d79d995455cab8dcd5b56d5a2fd |
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| 출처 메모 | uspto-grants-1987_11 |
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