Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Monochloramine → 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Monochloramine | HCID 25423 | — |
| 반응물 | alpha,2,6-Trimethylmorpholin-4-ylethanol | HCID 98999 | — |
| 생성물 | 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride | HCID 12955539 | — |
반응 단계
An amount, 389.3 grams, of 2,6-dimethyl-N-(2-hydroxypropyl) morpholine (2.25 moles) was condensed with the free chloroamine obtained from 481.5 grams N-chloroethyl-2,6-dimethylmorpholine hydrochloride (2.25 moles) as described above to give 415.9 grams (58.8%) of the catalyst, bp 127°-129° C. at 0.3 mm of Hg. The structure was confirmed as that of the title compound by elemental analysis, calc. 64.9 C, 10.9 H, 8.9 N; found 64.4 C, 10.6 H, 8.9 N.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04705840 |
| 출처 데이터셋 | uspto-grants-1987_11 |
| ORD ID | ord-2bf37e33554e4fd9b07d5dfa61613237 |
| 출처 메모 | uspto-grants-1987_11 |