Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 1-(Chloromethyl)-4-Ethoxybenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 4-Ethoxybenzyl alcohol | HCID 80345 | — |
| 생성물 | 1-(Chloromethyl)-4-Ethoxybenzene | HCID 2063971 | — |
반응 단계
4-Ethoxybenzyl alcohol (5 g) and concentrated hydrochloric acid (8.5 cm3) were vigorously stirred together for 30 minutes. The 2 phases were then allowed to separate, and the lower layer separated off, and diluted with chloroform. The organic solution was dried over anhydrous magnesium sulphate, and removal of the solvent by evaporation gave 4-ethoxybenzyl chloride (5.6 g). (This product is not stable on keeping, so was converted immediately to the phosphonium salt--see Example 12).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04705900 |
| 출처 데이터셋 | uspto-grants-1987_11 |
| ORD ID | ord-382b06ac20c74a1b8108fdcbcd7ddda9 |
| 출처 메모 | uspto-grants-1987_11 |