Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 3-Phenoxybenzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Benzenemethanol, 3-phenoxy-, 1-acetate | HCID 170904 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Phenoxybenzyl alcohol | HCID 26295 | 95% |
반응 단계
2.42 g. (0.01 mole) of 3-phenoxybenzyl acetate, 5 cm3. of methanol and 5 cm3. of 2N sodium hydroxide solution are refluxed for three hours. Then the methanol is distilled off and the organic phase is dissolved in 30 cm3. of methylene chloride, washed with 10 cm3. of 1N hydrochloric acid solution and 10 cm3. of water. 1.90 g. of 3-phenoxybenzyl alcohol are obtained. nD20 : 1.593, yield 95%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04709081 |
| 출처 데이터셋 | uspto-grants-1987_11 |
| ORD ID | ord-1a6f3bb1de714fc18ae39f93cc964184 |
| 출처 메모 | uspto-grants-1987_11 |