Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 3-Phenoxybenzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Benzenemethanol, 3-phenoxy-, 1-acetate | HCID 170904 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Phenoxybenzyl alcohol | HCID 26295 | 90% |
반응 단계
2.42 g. (0.01 mole) of 3-phenoxybenzyl acetate, 5 cm3. of methanol and 5 cm3. of 2N hydrochloric acid solution are refluxed for three hours. Then the methanol is distilled off. The organic phase is dissolved in 30 cm3. of methylene chloride, washed with 10 cm3. of water, 10 cm3. of 1N sodium hydroxide solution and 10 cm3. of water then evaporated. 1.8 g. of 3-phenoxybenzyl alcohol are obtained. nD20 : 1.593, yield 90%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04709081 |
| 출처 데이터셋 | uspto-grants-1987_11 |
| ORD ID | ord-f90801a985d04be688f6c4e70178ce4b |
| 출처 메모 | uspto-grants-1987_11 |