Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Hydroxy-2-naphthoic acid → 1,1,1-Trifluorooctan-2-YL 6-hydroxynaphthalene-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Hydroxy-2-naphthoic acid | HCID 85557 | — |
| 반응물 | 2-Octanol, 1,1,1-trifluoro- | HCID 97804 | — |
| 촉매 | Sulfuric Acid | HCID 1118 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1,1,1-Trifluorooctan-2-YL 6-hydroxynaphthalene-2-carboxylate | HCID 15724811 | — |
반응 단계
To a solution of 2-hydroxy-6-carboxynaphthalene (1 g) and optically active 1,1,1-trifluoro-2-octanol (1.1 g) in methylene chloride (50 ml) was added a few drops of conc. sulfuric acid and the mixture was refluxed under stirring for about two days.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05207947 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-43d063be546145bd9ec5526f7bbccb38 |
| 출처 메모 | uspto-grants-1993_05 |