Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Decanol → 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Decanol | HCID 8174 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 2-Dimethylaminopyridine | HCID 21885 | — |
| 반응물 | 2,6-Naphthalenedicarbonyl dichloride | HCID 3485596 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride | HCID 54316020 | 56.3% |
반응 단계
After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05207947 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-75e52ba2a4e54b1da4dfeb4197a82b67 |
| 출처 메모 | uspto-grants-1993_05 |