Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → HCID 19091417, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1-benzyl-N-methylpiperidin-4-amine | HCID 4136128 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 19091417 | HCID 19091417 | — |
반응 단계
0.2 mole of acetyl chloride is slowly added to a solution containing 0.2 mole of N-[1-(benzyl)-4-piperidyl]-N-methylamine, 0.2 mole of triethylamine and 500 cm3 of methylene chloride. The mixture is left in contact for 2 hours, evaporated, taken up in ether and then washed with water. After evaporation, an oil which corresponds to the expected compound is obtained:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208243 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-a477921d9c324c70a58a84057190fc6b |
| 출처 메모 | uspto-grants-1993_05 |