Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroethane → N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide dihydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroethane | HCID 6337 | — |
| 반응물 | N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide | HCID 9890945 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide dihydrochloride | HCID 19764599 | — |
반응 단계
5.5 g of the compound obtained in stage A is taken up in 10 cm3 of acetonitrile. 7.5 cm3 of a 3.3N solution of hydrochloric ether are added to this solution. 3.1 g of a solid which corresponds to the title compound are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208243 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-5e7f19ff56af4ccabb05d3f49423a133 |
| 출처 메모 | uspto-grants-1993_05 |