Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methylhydantoin → 5-[[4-Hydroxy-3,5-bis(1-methylethyl)phenyl]methylene]-1-methyl-2,4-imidazolidinedione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methylhydantoin | HCID 69217 | — |
| 반응물 | 4-Hydroxy-3,5-bis(isopropyl)benzaldehyde | HCID 82712 | — |
| 생성물 | 5-[[4-Hydroxy-3,5-bis(1-methylethyl)phenyl]methylene]-1-methyl-2,4-imidazolidinedione | HCID 54284051 | 11% |
반응 단계
Prepared according to the procedure described in Example 92 using 3,5-diisopropyl-4-hydroxybenzaldehyde (2.7 g, 13 mmoles) and 1-methyl hydantoin (1.4 g, 12 mmoles). Recrystallization from acetonitrile gave the pure product (0.4 g), mp 197°-208° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208250 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-aebed7088a92478092afa826da1265d1 |
| 출처 메모 | uspto-grants-1993_05 |