3-(Tetradecyloxy)benzoic acid → 3-(Tetradecyloxy)benzenemethanol

HRID 247934

반응식

HRID 247934 반응식
[CH2:1]([O:15][C:16]1[CH:17]=[C:18]([CH:22]=[CH:23][CH:24]=1)[C:19](O)=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH2:1]([O:15][C:16]1[CH:17]=[C:18]([CH2:19][OH:20])[CH:22]=[CH:23][CH:24]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

참가 물질

4

반응물 2

HCID 32623113-(Tetradecyloxy)benzoic acidHCID 21226445Aluminium lithium hydride

생성물 1

HCID 100417103-(Tetradecyloxy)benzenemethanol

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The title compound is prepared by the procedure of Example 21 using 20.0 g of product from Example 23, 200 ml of dry tetrahydrofuran and 7.94 g of lithium aluminum hydride. The product, 18.82 g, is obtained as colorless crystals.

후처리

  1. customThe product, 18.82 g, is obtained as colorless crystals

출처 및 근거

ORD 기록
ord-ca8b5851690a4d12bf55b9d8299cf440
출처 데이터셋
uspto-grants-1993_05
특허 번호
US05208247

연결된 노트

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