Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → p-Tetradecyloxyphenylacetylchloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | p-Tetradecyloxyphenylacetic acid | HCID 10472964 | — |
| 촉매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | p-Tetradecyloxyphenylacetylchloride | HCID 10021844 | 100% |
반응 단계
To a mixture of 60.6 g of product from Example 52 in 750 ml of methylene chloride and 0.636 g of dimethylformamide is added, dropwise, 33.1 g of oxalyl chloride. The reaction is stirred at room temperature for 18 hours. The mixture is concentrated in vacuo, redissolved in diethyl ether, passed through a pad of diatomaceous earth and concentrated in vacuo to give 63.81 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208247 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-7dd389b6a302427da4a75e6d768645eb |
| 출처 메모 | uspto-grants-1993_05 |