4-Methylbenzenethiol → HCID 19764849, 화합물

HRID 248094

반응식

[C:1]1([CH3:8])[CH:6]=[CH:5][C:4]([SH:7])=[CH:3][CH:2]=1.[Br:9][C:10]1[CH:15]=[C:14]([C:16]([F:19])([F:18])[F:17])[CH:13]=[C:12](F)[CH:11]=1>>[C:1]1([CH3:8])[CH:6]=[CH:5][C:4]([S:7][C:12]2[CH:13]=[C:14]([C:16]([F:18])([F:17])[F:19])[CH:15]=[C:10]([Br:9])[CH:11]=2)=[CH:3][CH:2]=1

참가 물질

반응물 2

HCID 78114-Methylbenzenethiol

HCID 27363233-Bromo-5-fluorobenzotrifluoride

생성물 1

HCID 19764849HCID 19764849, 화합물수율 63%

실험 절차

Using a similar procedure to that described in the 1st paragraph of Note a. above 4-toluenethiol was reacted with 1-bromo-3-fluoro-5-trifluoromethylbenzene to give 3-bromo-5-trifluoromethylphenyl 4-tolyl sulphide in 63% yield as an oil.

출처 및 근거

ORD 기록: ord-bdb4bed397164cd9a7fef44ca74741dc
출처 데이터셋: uspto-grants-1993_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05208259

연결된 노트

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