Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Naphthol → HCID 53988552, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Naphthol | HCID 7005 | — |
| 반응물 | (2R)-Oxiran-2-ylmethyl butanoate | HCID 2724536 | — |
| 촉매 | Tetrabutylammonium Iodide | HCID 67553 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 53988552 | HCID 53988552 | 75% |
반응 단계
To a solution of 144 g (1 mol) of 1-naphthol and 7.4 g (0.02 mol) of tetrabutylammonium iodide in 200 ml of toluene was added 144 g (1 mol) of (R)-glycidyl butyrate over a period of 15 min at a temperature of 120° C., and the mixture was kept at this temperature for a further 4 h. Conventional subsequent treatment of the reaction mixture gave the required compound as an oil, yield about 75%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208333 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-86e317ef3b474747a22b6fcc78057d05 |
| 출처 메모 | uspto-grants-1993_05 |