Toluene → HCID 178439713, 화합물

HRID 248310노트

반응식

HRID 248310 반응식
[F:1][C:2]([F:12])([F:11])[C@H:3]1[CH2:8][CH2:7][C@H:6]([CH:9]=[O:10])[CH2:5][CH2:4]1.[CH2:13]([CH:16]([CH3:20])[CH:17](O)[OH:18])[CH2:14][CH3:15].C1(C)C=CC=CC=1.CC1C=CC(S(O)(=O)=O)=CC=1>O>[F:1][C:2]([F:11])([F:12])[C@H:3]1[CH2:4][CH2:5][C@H:6]([CH:9]2[O:18][CH2:17][CH:16]([CH2:13][CH2:14][CH3:15])[CH2:20][O:10]2)[CH2:7][CH2:8]1

참가 물질

6

반응물 4

HCID 1140TolueneHCID 6101p-Toluenesulfonic acidHCID 219438382-PropylpropanediolHCID 178520943HCID 178520943, 화합물

생성물 1

HCID 178439713HCID 178439713, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A mixture of 0.02 mol of trans-4-trifluoromethyl-1-formylcyclohexane (prepared as in Example 3), 0.02 mol of 2-propylpropanediol, 30 ml of toluene and 0.5 g of pTsOH (sic) is heated for 4 hours on a water separator. The pure product is obtained after customary work-up and crystallization.

후처리

  1. customThe pure product is obtained
  2. customafter customary work-up and crystallization

출처 및 근거

ORD 기록
ord-08f48b11c11f42c2b6f50a89daae7568
출처 데이터셋
uspto-grants-1993_05
특허 번호
US05209868

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