Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → (3Z)-3-[[4-(morpholin-4-ylmethyl)anilino]-phenylmethylidene]-5-nitro-1H-indol-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 4-(Morpholinomethyl)aniline | HCID 776851 | — |
| 반응물 | 1-Acetyl-3-{1-ethoxy-1-phenylmethylidene}-5-nitro-2-indolinone | HCID 54280104 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | (3Z)-3-[[4-(morpholin-4-ylmethyl)anilino]-phenylmethylidene]-5-nitro-1H-indol-2-one | HCID 178517274 | — |
반응 단계
Prepared analogously to Example 82 from 1-acetyl-3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone and 4-morpholinomethyl-aniline in DMF and subsequent treatment with sodium hydroxide solution in methanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06855710B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-b5062f56dc5e453b9cebe08f1cbeadce |
| 출처 메모 | uspto-grants-2005_02 |