Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroacetic Acid → 2-(2,5-Dichlorophenyl)-2-mercaptoacetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroacetic Acid | HCID 300 | — |
| 반응물 | 2,5-Dichloroaniline | HCID 7262 | — |
| 반응물 | 2,5-Dichlorobenzenethiol | HCID 79965 | — |
| 반응물 | Thiourea | HCID 2723790 | — |
| 촉매 | Copper Sulfate | HCID 24462 | — |
| 생성물 | 2-(2,5-Dichlorophenyl)-2-mercaptoacetic acid | HCID 22492329 | — |
반응 단계
the method in which 2,5-dichloroaniline is diazotized and then reacted with thiourea in the presence of copper sulfate and subsequently hydrolyzed to 2,5-dichlorothiophenol, followed by reaction with monochloroacetic acid to yield 2,5-dichlorophenylthioglycolic acid (Ger. Offen. DE3715508),
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05210287 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-87f5429d54f94a869a229441326f3c7f |
| 출처 메모 | uspto-grants-1993_05 |