Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Carbonate → Diethylene glycol diethyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Carbonate | HCID 7766 | — |
| 반응물 | Diethylene Glycol Monoethyl Ether | HCID 8146 | — |
| 반응물 | Aluminum | HCID 5359268 | — |
| 반응물 | Magnesium | HCID 5462224 | — |
| 생성물 | Diethylene glycol diethyl ether | HCID 8179 | — |
반응 단계
A mixture of 2-(2-ethoxyethoxy)ethanol (1 mole) and diethyl carbonate (3 mole) was passed through 11.5 grams of a magnesium:aluminum mixed metal oxide (3/16 inch pellets, Mg/Al 3:1) at a temperature of 225° C. and at a liquid feed rate of 0.29 milliliters/minute. After a period of one hour, a total of 30.2 grams of liquid was collected. Analysis was performed by capillary gas chromatography (FID) using a DB-1701 column. The results were (area %) as follows:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05210322 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-528009b6826c405d946c3525eea95ba5 |
| 출처 메모 | uspto-grants-1993_05 |