Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl Peroxide → 2-Bromoethyl Benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 2-Phenyl-1,3-dioxolane | HCID 70293 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 2-Bromoethyl Benzoate | HCID 523090 | — |
반응 단계
A mixture of 120.14 grams (0.80 mol) of 2-phenyl-1,3-dioxolane, 142.39 grams (0.80 mol) of N-bromosuccinimide, 1 liter of carbon tetrachloride and a catalytic amount of benzoyl peroxide was heated with stirring at reflux for 5.25 hours and then cooled. The mixture was filtered, and the filtrate was concentrated to an oil. Distillation of this oil gave 147.8 grams; (80.65% of theory) of the product; bp=104°-111° C./0.40 mm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05212035 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-1044f04a15c24fb09d0e70d2d8fc00f4 |
| 출처 메모 | uspto-grants-1993_05 |