Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → N-(2-benzoyloxyethyl)pyridinium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | 2-Bromoethyl Benzoate | HCID 523090 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-(2-benzoyloxyethyl)pyridinium bromide | HCID 19762119 | — |
반응 단계
A solution of 50.0 grams (0.218 mol) of 2-bromoethyl benzoate, 17.27 grams (0.218 mol) of pyridine and 135 milliters of acetonitrile was heated at reflux for 17.75 hours and cooled. Solid crystallized and was collected, washed with acetonitrile, then with ether and dried. The yield of product was 48.5 grams (72.19% of theory); mp=162°-164° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05212035 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-411144a61709494ca8c92627bc98e1d5 |
| 출처 메모 | uspto-grants-1993_05 |