Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Tetraphenylborate → N-(2-Acetyloxyethyl)pyridinium Tetraphenylborate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Tetraphenylborate | HCID 2723787 | — |
| 반응물 | N-(2-Acetyloxyethyl)-pyridinium Bromide | HCID 19762112 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(2-Acetyloxyethyl)pyridinium Tetraphenylborate | HCID 19762114 | — |
반응 단계
To a solution of 24.61 grams (0.10 mol) of N-(2-acetyloxyethyl)pyridinium bromide in 250 milliters of water there was added a solution of 34.24 grams (0.10 mol) of sodium tetraphenylborate in 150 milliters of water. An oily precipitate formed which was treated with 500 milliters of water to give a white solid. The solid was collected and recrystallized from acetonitrile. The yield of product was 39.8 grams (81.99 % of theory); mp=223°-224° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05212035 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-16349dba04d647b7967b8f55725171d1 |
| 출처 메모 | uspto-grants-1993_05 |