Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → N,N-dimethyl-2-(4-nitrophenoxy)ethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | 1-(2-Bromoethoxy)-4-nitrobenzene | HCID 235987 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | N,N-dimethyl-2-(4-nitrophenoxy)ethanamine | HCID 887421 | — |
반응 단계
4.9 g (20 mmol) of 4-(2-bromoethyloxy)-nitrobenzene and 2.7 g (60 mmol) of dimethylamine in 50 ml of dimethylformamide are heated to 100° C. for 24 hours in a bomb tube. After removal of the solvent in vacuo the residue is taken up in water and extracted with dichloromethane. The organic phase is dried and concentrated by evaporation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06855710B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-a8e4bf5abd1e4934998ac18b605dab70 |
| 출처 메모 | uspto-grants-2005_02 |