HCID 67653663, 화합물 → Morpholine, 4-(2-methoxyethyl)-

HRID 249418노트

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HRID 249418 반응식
[CH3:1][O:2][C:3](=O)O.OC[CH2:8][N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1>C1CCCCC1>[CH3:13][O:12][CH2:11][CH2:10][N:9]1[CH2:14][CH2:1][O:2][CH2:3][CH2:8]1

참가 물질

3

반응물 1

HCID 67653663HCID 67653663, 화합물

생성물 1

HCID 82460Morpholine, 4-(2-methoxyethyl)-

시약·촉매·용매 1

HCID 8078Cyclohexane용매

실험 절차

Using the apparatus employed in Examples 15-27, a 20 percent (volume) solution of 4-(2-hydroxyethyl)morpholine methyl carbonate Prepared in Example 30 in cyclohexane was passed through 6.0 grams of Catalyst J at a temperature of 300° C. and a liquid feed rate of 0.27 milliliters per minute. A total of 7.4 grams of product was recovered. Capillary gas chromatographic analysis (area percent) of this material showed 67.7 percent selectivity to 4-(2-methoxyethyl)morpholine at 100 percent 4-(2-hydroxyethyl)morpholine methyl carbonate conversion.

후처리

  1. customA total of 7.4 grams of product was recovered

출처 및 근거

ORD 기록
ord-c1e58d64c5f349b197d5d363145da678
출처 데이터셋
uspto-grants-1993_05
특허 번호
US05214142

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