Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(4-Nitrophenyl)butyric acid → 2-(4-Aminophenyl)butanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(4-Nitrophenyl)butyric acid | HCID 24047 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-(4-Aminophenyl)butanoic acid | HCID 34655 | 92% |
반응 단계
A solution of 2-(4'-nitrophenyl)butyric acid (6.99 g, 33.4 mmol) in 250 mL of EtOH and 0.5 g of 10% Pd-C was hydrogenated overnight at 55 psi. The solution was filtered and evaporated under vacuum to give 5.50 g (92%) of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05214191 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-a9c1d3d2d2a743a29e28daf310be9010 |
| 출처 메모 | uspto-grants-1993_05 |