참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethyl Lactate | HCID 7344 | — |
| 반응물 | 3,7-Dimethyl-1-octanol | HCID 7792 | — |
| 생성물 | 3,7-Dimethyl-1-octyl lactate | HCID 11535958 | 62.2% |
반응 단계
A mixture of Novozym 435 (2.81 g), molecular sieves (23.17 g), 3,7-dimethyl-1-octanol (4.64 g), and ethyl lactate (14.78 g) in a 250 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.2 g of 3,7-dimethyl-1-octyl lactate (62% yield) was obtained as an amber-colored liquid. The purity of the product was >96% as assessed by HPLC-RI.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07863025B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_01 |
|---|
| ORD ID | ord-5ef4352b11c3443e87db73d3185b8e02 |
|---|
| 출처 메모 | uspto-grants-2011_01 |
|---|
