Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenylhydrazine → HCID 178515184, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenylhydrazine | HCID 7516 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethyl 4-Chloroquinoline-3-carboxylate | HCID 268963 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | HCID 178515184 | HCID 178515184 | — |
반응 단계
A suspension of ethyl 4-chloro-quinoline-3-carboxylate (3a) (2.35 g, 0.01 M) in 20 mL of o-xylene was refluxed with triethylamine (2.0 mL, 0.02 M) and phenyl hydrazine (2.89 g, 0.02 M) overnight. The crude product was obtained by filtration followed by washing the solid with cold methanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07863266B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-14d96c75fdcb4a85a34f10dc3a1a4f64 |
| 출처 메모 | uspto-grants-2011_01 |