Phenylhydrazine → HCID 178515184, 화합물

HRID 249668

반응식

HRID 249668 반응식
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][C:3]=1[C:12]([O:14]CC)=O.C(N(CC)CC)C.[C:24]1([NH:30][NH2:31])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>CC1C=CC=CC=1C>[C:24]1([N:30]2[C:12](=[O:14])[C:3]3=[CH:4][NH:5][C:6]4[CH:7]=[CH:8][CH:9]=[CH:10][C:11]=4[C:2]3=[N:31]2)[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1

참가 물질

5

반응물 3

HCID 7516PhenylhydrazineHCID 8471TriethylamineHCID 268963Ethyl 4-Chloroquinoline-3-carboxylate

생성물 1

HCID 178515184HCID 178515184, 화합물

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

A suspension of ethyl 4-chloro-quinoline-3-carboxylate (3a) (2.35 g, 0.01 M) in 20 mL of o-xylene was refluxed with triethylamine (2.0 mL, 0.02 M) and phenyl hydrazine (2.89 g, 0.02 M) overnight. The crude product was obtained by filtration followed by washing the solid with cold methanol.

출처 및 근거

ORD 기록
ord-14d96c75fdcb4a85a34f10dc3a1a4f64
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07863266B2

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