3-(4-Methoxyphenyl)propylazide → 3-(4-Methoxyphenyl)propan-1-amine

반응식

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][N:12]=[N+]=[N-])=[CH:5][CH:4]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][NH2:12])=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 117153263-(4-Methoxyphenyl)propylazide

HCID 21226445Aluminium lithium hydride

생성물 1

HCID 30298153-(4-Methoxyphenyl)propan-1-amine

실험 절차

Amine 13 was prepared as described in procedure A from azide 12 (5.2 g, 0.027 mol) and LAH (26 ml of 1 M solution in THF).

출처 및 근거

ORD 기록: ord-c8cc28f18c9443a2981ce665cdcd0af1
출처 데이터셋: uspto-grants-2005_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06858614B2

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