Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(4-Aminobutyl)-N-methyl carbamic acid tert-butyl ester → {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(4-Aminobutyl)-N-methyl carbamic acid tert-butyl ester | HCID 2756377 | — |
| 반응물 | Sodium triacetoxyborohydride | HCID 5049666 | — |
| 반응물 | 3,5-Dimethylpyridine-2-carbaldehyde | HCID 18731683 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester | HCID 58997083 | — |
반응 단계
Using General Procedure B: Reaction of (4-Amino-butyl)-methyl-carbamic acid tert-butyl ester and 3,5-dimethyl-pyridine-2-carbaldehyde with NaBH(OAc)3 in CH2Cl2 gave {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07863293B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-cc4bc05c439d4badafba0393c2085ef4 |
| 출처 메모 | uspto-grants-2011_01 |