Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → Methyl 5-acetyl-2-methoxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Cesium carbonate | HCID 10796 | — |
| 반응물 | Methyl 5-acetylsalicylate | HCID 85444 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl 5-acetyl-2-methoxybenzoate | HCID 606426 | — |
반응 단계
To a stirred solution of Methyl 2-hydroxy-5-acetylbenzoate (12 g, 61.7 mmol) in DMF (200 ml) was added cesium carbonate (24.15 g, 74.1 mmol) and MeI (9.64 g, 68 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07863475B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-6cb3c30c25e643ff968fd64e2986f8ec |
| 출처 메모 | uspto-grants-2011_01 |