Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 5-(1-Chlorobutyl)-2-(2,6-diethyl-phenyl)-4-ethoxy-pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 1-[6-(2,6-Diethyl-phenyl)-4-ethoxy-pyridin-3-yl]-butan-1-ol | HCID 59678316 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 5-(1-Chlorobutyl)-2-(2,6-diethyl-phenyl)-4-ethoxy-pyridine | HCID 66993937 | — |
반응 단계
A mixture of 1-[6-(2,6-diethyl-phenyl)-4-ethoxy-pyridin-3-yl]-butan-1-ol (29 mg) and SOCl2 (0.2 mL) in CH2Cl2 (1 ml) is stirred at room-temperature for one hour. The volatile materials are removed in vacuo to give 5-(1-chlorobutyl)-2-(2,6-diethyl-phenyl)-4-ethoxy-pyridine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07863454B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-eb2032ddbdcc473494e4fbec3c2ae06e |
| 출처 메모 | uspto-grants-2011_01 |