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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 251931생성일: 2026년 10월 26일

Dimethylformamide → 2-Amino-5-chloro-3-methoxybenzoic acid

https://huagongshe.com/reaction/251931

반응식

참여 물질

역할이름HCID투입량
반응물DimethylformamideHCID 6228—
반응물ChlorosuccinimideHCID 31398—
반응물2-Amino-3-methoxybenzoic acidHCID 255720—
용매WaterHCID 962—
생성물2-Amino-5-chloro-3-methoxybenzoic acidHCID 5459587461.1%

반응 단계

To a mixture of 1.67 g of 2-amino-3-methoxybenzoic acid and 100 ml of N,N-dimethylformamide was added 1.3 g of N-chlorosuccinimide at room temperature, and the resulting mixture was stirred at room temperature for 10 hours. Water was poured into the reaction mixture, and a deposited precipitate was collected by filtration to obtain 1.2 g of 2-amino-5-chloro-3-methoxybenzoic acid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07867949B2
출처 데이터셋uspto-grants-2011_01
ORD IDord-07d6ef35f3d041359215050c38ce936e
출처 메모uspto-grants-2011_01