반응식
[C:1]([OH:5])(=[O:4])[C:2]#[CH:3].[N:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[N+:7]=[N-:8]>>[CH2:9]([N:6]1[CH:3]=[C:2]([C:1]([OH:5])=[O:4])[N:8]=[N:7]1)[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]참가 물질
3
반응 조건
- 온도
- 120 °C
실험 절차
A mixture of propiolic acid (46 μL, 0.7419 mmol) and 1-azido-dodecane (156.8 mg, 0.7419 mmol) was heated to 120° C. in a capped vial for 14 h, to yield the title triazole as white, crystalline solid (189.3 mg, 91% yield). The product was used without further purification.
출처 및 근거
- ORD 기록
- ord-eb3be02f342142e3bc24729ff2e33713
- 출처 데이터셋
- uspto-grants-2011_01
- 특허 번호
- US07868135B2
연결된 노트
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