(4-Chlorophenyl)hydrazine → HCID 178515231, 화합물

HRID 252955

반응식

HRID 252955 반응식
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]2[C:8]3[C:9]([C:14](=[O:23])[N:15]([C:17]4[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=4)[N:16]=3)=[CH:10][NH:11][C:12]=2[CH:13]=1)([O-:3])=[O:2].[Cl:24]C1C2C(=CC([N+]([O-])=O)=CC=2)N=CC=1C(OCC)=O.ClC1C=CC(NN)=CC=1>>[Cl:24][C:20]1[CH:21]=[CH:22][C:17]([N:15]2[C:14](=[O:23])[C:9]3=[CH:10][NH:11][C:12]4[CH:13]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=[CH:6][C:7]=4[C:8]3=[N:16]2)=[CH:18][CH:19]=1

참가 물질

4

반응물 3

HCID 70624(4-Chlorophenyl)hydrazineHCID 21303360Ethyl 4-chloro-7-nitroquinoline-3-carboxylateHCID 178515230HCID 178515230, 화합물

생성물 1

HCID 178515231HCID 178515231, 화합물

실험 절차

The title compound was prepared following the procedure described for 12a using 11a and 4-chlorophenylhydrazine. 1H-NMR (DMSO-d6) δ (ppm): 7.48 (2H, d, m), 8.20 (2H, m), 8.26 (1H, dd, J=8.61, 2.08 Hz), 8.40 (1H, d, J=8.61 Hz), 8.52 (1H, d, J=2.08 Hz), 8.92 (1H, s). m/z 341.8 (MH+).

출처 및 근거

ORD 기록
ord-f2c3b7ec83184651aae27706f175bf7c
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07872002B2

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