Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitroindazole → NoName_3327
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitroindazole | HCID 18057 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | NoName_3327 | HCID 413085 | 101.3% |
반응 단계
A mixture of 4-nitro-1H-indazole (760 mg, 4.68 mmol), palladium on charcoal (10%, cat.) and ethanol (30 mL) was stirred under a balloon of hydrogen for 4 hours. The reaction mixture was then filtered through celite, and the solvent removed in vacuo to yield 1H-indazol-4-ylamine (68) (631 mg, 100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07872003B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-fa3777e0d9a04dadb1f178fb5c3866d4 |
| 출처 메모 | uspto-grants-2011_01 |