4-Methoxybenzaldehyde → 2-(4-Methoxyphenyl)-4-iodomethyl-5-methyloxazole

HRID 253348

반응식

HRID 253348 반응식
[I:1][CH2:2][C:3]1[N:4]=[C:5]([C:14]2[CH:19]=[CH:18][C:17](C)=[CH:16][CH:15]=2)[O:6][C:7]=1[C:8]1C=CC=CC=1.C/C(/[C:25](C)=[O:26])=N\O.COC1C=CC(C=O)=CC=1>>[I:1][CH2:2][C:3]1[N:4]=[C:5]([C:14]2[CH:19]=[CH:18][C:17]([O:26][CH3:25])=[CH:16][CH:15]=2)[O:6][C:7]=1[CH3:8]

참가 물질

4

반응물 3

HCID 312444-MethoxybenzaldehydeHCID 64096332,3-Butanedione monoximeHCID 574345044-Iodomethyl-5-phenyl-2-p-tolyloxazole

생성물 1

HCID 224936592-(4-Methoxyphenyl)-4-iodomethyl-5-methyloxazole

실험 절차

Analogously to the building block synthesis of 4-iodomethyl-5-phenyl-2-p-tolyloxazole, diacetylmonoxime and 4-methoxybenzaldehyde gave 4-iodomethyl-2-(4 methoxyphenyl)-5-methyloxazole.

출처 및 근거

ORD 기록
ord-94c0a80e2e3746b2a8971466f2b3c9ee
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07872034B2

연결된 노트

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