3-Methylbenzaldehyde → 4-Iodomethyl-5-methyl-2-m-tolyloxazole

HRID 253351

반응식

HRID 253351 반응식
[I:1][CH2:2][C:3]1[N:4]=[C:5]([C:14]2[CH:19]=[CH:18][C:17](C)=[CH:16][CH:15]=2)[O:6][C:7]=1[C:8]1C=CC=CC=1.[CH3:21]/C(/C(C)=O)=N\O.C1(C)C=CC=C(C=O)C=1>>[I:1][CH2:2][C:3]1[N:4]=[C:5]([C:14]2[CH:15]=[C:16]([CH3:21])[CH:17]=[CH:18][CH:19]=2)[O:6][C:7]=1[CH3:8]

참가 물질

4

반응물 3

HCID 121053-MethylbenzaldehydeHCID 64096332,3-Butanedione monoximeHCID 574345044-Iodomethyl-5-phenyl-2-p-tolyloxazole

생성물 1

HCID 219803084-Iodomethyl-5-methyl-2-m-tolyloxazole

실험 절차

Analogously to the building block synthesis of 4-iodomethyl-5-phenyl-2-p-tolyloxazole, diacetylmonoxime and m-tolualdehyde gave 4-iodomethyl-5-methyl-2-m-tolyloxazole.

출처 및 근거

ORD 기록
ord-f2dd0a24647f4d6c9cf3b071bf60cfd5
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07872034B2

연결된 노트

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