1-Phenylcyclohexane-1-carboxylic acid → HCID 178441257, 화합물

HRID 253638

반응식

HRID 253638 반응식
[C:1]([N:5]1[CH:9]=[C:8]([CH2:10][CH2:11][CH2:12][CH3:13])[C:7](=[NH:14])[S:6]1)([CH3:4])([CH3:3])[CH3:2].[C:15]1([C:21]2([C:27](O)=[O:28])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH2:10]([C:8]1=[CH:9][N:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[S:6]/[C:7]/1=[N:14]\[C:27]([C:21]1([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1)=[O:28])[CH2:11][CH2:12][CH3:13]

참가 물질

3

반응물 2

HCID 708171-Phenylcyclohexane-1-carboxylic acidHCID 668672282-tert-Butyl-4-butylisothiazol-5(2H)-imine

생성물 1

HCID 178441257HCID 178441257, 화합물

실험 절차

The product from Example 92B and 1-phenylcyclohexanecarboxylic acid (Aldrich) were processed using the method described in Example 92C to afford the title compound. 1H NMR (DMSO-d6) δ 0.90 (t, J=7.3 Hz, 3H), 1.20-1.77 (m, 21H), 2.61-2.69 (m, 4H), 7.10-7.15 (m, 1H), 7.21-7.27 (m, 2H), 7.35-7.39 (m, 2H), 8.51 (s, 1H). MS (ESI+) m/z 399 (M+H)+. Anal. calcd. for C24H34N2OS: C, 72.32; H, 8.60; N, 7.03. Found: C, 72.24; H, 8.59; N, 7.10.

출처 및 근거

ORD 기록
ord-5341ab7474bb4d7aa029ebe8a0407a03
출처 데이터셋
uspto-grants-2011_01
특허 번호
US07872033B2

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