Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → ethyl (NZ)-N-[4-butyl-2-(1,1,1-trifluoro-2-methylpropan-2-yl)-1,2-thiazol-5-ylidene]carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | Hexanal | HCID 6184 | — |
| 반응물 | Ethyl isothiocyanatoformate | HCID 85320 | — |
| 반응물 | 1,1,1-Trifluoro-2-methylpropan-2-amine | HCID 11275188 | — |
| 생성물 | ethyl (NZ)-N-[4-butyl-2-(1,1,1-trifluoro-2-methylpropan-2-yl)-1,2-thiazol-5-ylidene]carbamate | HCID 87184182 | — |
반응 단계
Commercially available hexanal (Aldrich), 1,1,1-trifluoro-2-methylpropan-2-amine (Chemcollect), O-ethyl carbonisothiocyanatidate (Aldrich) and iodine were processed using the method described in Example 110A to afford the title compound. MS (ESI+) m/z 339 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07872033B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-4288e9071d894b849c100c13d51a098f |
| 출처 메모 | uspto-grants-2011_01 |